Issue

Vol. 18 (2026)

Decoding Hydrogen-Bond Network of Electrolyte for Cryogenic Durable Aqueous Zinc-Ion Batteries

https://doi.org/10.1007/s40820-025-01970-3
Xiyan Wei
Shenzhen Key Laboratory of Advanced Energy Storage, Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China
Jinpeng Guan
Shenzhen Key Laboratory of Advanced Energy Storage, Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China
Yongbiao Mu
Shenzhen Key Laboratory of Advanced Energy Storage, Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China
Yuhan Zou
College of Energy, Soochow Institute for Energy and Materials Innovations, Key Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu Province, Soochow University, Suzhou 215006, People’s Republic of China
Xianbin Wei
Department of Materials Science and Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China
Lin Yang
Shenzhen Key Laboratory of Advanced Energy Storage, Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China
Quanyan Man
Shenzhen Key Laboratory of Advanced Energy Storage, Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China
Chao Yang
MOE Key Laboratory of New Processing Technology for Nonferrous Metal and Materials, Key Laboratory of Natural and Biomedical Polymer Materials (Education Department of Guangxi Zhuang Autonomous Region), College of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, People’s Republic of China
Limin Zang
MOE Key Laboratory of New Processing Technology for Nonferrous Metal and Materials, Key Laboratory of Natural and Biomedical Polymer Materials (Education Department of Guangxi Zhuang Autonomous Region), College of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, People’s Republic of China
Jingyu Sun
College of Energy, Soochow Institute for Energy and Materials Innovations, Key Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu Province, Soochow University, Suzhou 215006, People’s Republic of China
Lin Zeng
Shenzhen Key Laboratory of Advanced Energy Storage, Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, People’s Republic of China

Corresponding Author: Lin Zeng

zengl3@sustech.edu.cn

Nano-Micro Letters, Vol. 18 (2026), Article Number: 127

Abstract

Aqueous zinc-ion batteries (AZIBs) hold great promise for next-generation energy storage but face challenges such as Zn dendrite growth, side reactions, and limited performance at low temperatures. Here, we propose an electrolyte design strategy that reconstructs the hydrogen-bond network through the synergistic effect of glycerol (GL) and methylsulfonamide (MSA), enabling the formation of a (100)-oriented Zn anode. This design significantly broadens the operating current and temperature windows of AZIBs. As a result, Zn||Zn symmetric cells exhibit remarkable cycling stability, achieving 4,000 h at 1 mA cm−2 and 600 h at 40 mA cm−2 (both at 1 mAh cm−2 capacity); even at −20 °C, Zn||Zn symmetric cells deliver ultra-stable cycling for over 5,400 h. Furthermore, Zn||VO2 full cells retain 77.3% of their capacity after 2,000 cycles at 30 °C with a current density of 0.5 A g−1 and 85.4% capacity retention after 2,000 cycles at −20 °C and 0.25 A g−1. These results demonstrate a robust pathway for enhancing the practicality and low-temperature adaptability of AZIBs.


Highlights:
1 The hydrogen-bond network structure and solvation structure of the electrolyte are reconstructed by glycerol (GL) and methylsulfonamide (MSA) to achieve low-temperature durability in aqueous zinc-ion batteries (AZIBs).
2 GL and MSA collaboratively construct (100)-oriented high-activity dendrite-free zinc anode to improve the rate performance of AZIBs.
3 The Zn||Zn symmetrical cell achieved stable operation for 4,000 h at 1 mA cm−2 and 1 mAh cm−2 (30 °C) and 5,400 h at 0.5 mA cm−2 and 0.5 mAh cm−2 (−20 °C).

Keywords

Aqueous zinc-ion batteries Electrolyte additive Hydrogen-bond reconstruction High-rate performance Low temperature
Wei, Xiyan, Jinpeng Guan, Yongbiao Mu, Yuhan Zou, Xianbin Wei, Lin Yang, Quanyan Man, Chao Yang, Limin Zang, Jingyu Sun, and Lin Zeng. 2026. “Decoding Hydrogen-Bond Network of Electrolyte for Cryogenic Durable Aqueous Zinc-Ion Batteries”. Nano-Micro Letters 18 (January):127. https://doi.org/10.1007/s40820-025-01970-3.
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